更精準(zhǔn)操作鹽霧試驗(yàn)機(jī)【美國(guó)Q-Lab】

發(fā)布時(shí)間：2012.11.30 新聞來(lái)源：【翁開爾集團(tuán)】瀏覽次數(shù)：

鹽霧試驗(yàn)是一種主要利用鹽霧試驗(yàn)設(shè)備所創(chuàng)造的人工模擬鹽霧環(huán)境條件來(lái)考核產(chǎn)品或金屬材料耐腐蝕性能的環(huán)境試驗(yàn)。那么如何操作鹽霧試驗(yàn)機(jī)才能使試驗(yàn)結(jié)果更精準(zhǔn)？

（1）鹽霧試驗(yàn)機(jī)基本組成和工作原理

目前國(guó)內(nèi)外普遍采用的試驗(yàn)沒備是鹽霧試驗(yàn)機(jī)。該設(shè)備主要由鹽霧箱體(噴霧室)、鹽溶液貯槽、鹽溶液的液位控制器、經(jīng)由適當(dāng)處理的壓縮空氣系統(tǒng)、一個(gè)或多個(gè)霧化噴嘴中心噴霧塔、可調(diào)式折流板、樣板支架(滿足與垂線的夾角是(20±5°的支撐板)、空氣飽和器、箱體浸沒式加熱設(shè)備及必要的溫度、濕度控制設(shè)備等組成。當(dāng)鹽溶液自溶液貯槽內(nèi)導(dǎo)出流經(jīng)液位控制器進(jìn)入噴霧塔底部時(shí)，在一定壓力的氣流(壓差)作用下，自由吸式噴嘴吸人并霧化形成密集的鹽霧，經(jīng)噴霧塔上部的折流板導(dǎo)向噴出后均勻地沉降在噴霧室內(nèi)的試驗(yàn)樣板上。儀器的結(jié)構(gòu)應(yīng)能保證積聚在頂堋或箱蓋上的滴液不會(huì)滴在試驗(yàn)樣板上。試驗(yàn)樣板上的滴液也不會(huì)滴落到溶液貯槽內(nèi)重新霧化。該設(shè)備除了能完成中性鹽霧試驗(yàn)外，對(duì)于醋酸-鹽霧試驗(yàn)、銅加速的醋酸-鹽霧試驗(yàn)（CASS試驗(yàn)）只要按標(biāo)準(zhǔn)在鹽溶液中加入醋酸或氯化銅與醋酸，并改變相應(yīng)的試驗(yàn)條件，就可在普通的鹽霧試驗(yàn)箱進(jìn)行。

循環(huán)鹽霧試驗(yàn)機(jī)是為滿足濕（鹽霧）/干燥/濕氣—循環(huán)腐蝕環(huán)境試驗(yàn)而設(shè)計(jì)的。該設(shè)備除了具備普通鹽霧試驗(yàn)箱的所有構(gòu)成外，又要增加可控溫度的干熱空氣鼓風(fēng)機(jī)及干燥空氣（提供相對(duì)濕度為20%到30%之間及相對(duì)濕度(50±20)%的去油去塵空氣）供給器，還有一個(gè)可編程的程序控制器。以便對(duì)試驗(yàn)箱內(nèi)分別設(shè)置完成如噴鹽霧、送干燥熱風(fēng)、送接近飽和的濕空氣或半飽和的濕空氣的循環(huán)程序。

（2）試驗(yàn)參數(shù)設(shè)定

溫度控制

耐中性鹽霧試驗(yàn)及醋酸—鹽霧試驗(yàn)的鹽霧箱曝露區(qū)的溫度應(yīng)保持在(35±2)℃?？諝怙柡推鞯臏囟葢?yīng)高于箱內(nèi)溫度(5~10)℃。用于醋酸／銅加速—鹽霧試驗(yàn)的鹽霧箱曝露區(qū)的溫度應(yīng)保持在(49±1)℃。

鹽霧沉降量的控制

在鹽霧機(jī)曝露區(qū)內(nèi)至少應(yīng)有兩個(gè)干凈的由玻璃或其他化學(xué)惰性材料制成的鹽霧收集器，其中一個(gè)應(yīng)放在噴霧入口附近，另外一個(gè)放在遠(yuǎn)離噴霧入口處。鹽霧沉降量：在最少24h周期后，開始計(jì)算所收集的溶液，每80cm2的收集器面積每小時(shí)應(yīng)收集到1.0~2.0ml的鹽溶液，其氯化鈉溶液的濃度為5％(質(zhì)量)，PH值應(yīng)為6.5~7.5。

溶液配制

A.中性鹽霧溶液的配制。

將符合GBl266化學(xué)純的氯化鈉溶解于符合GB6682三級(jí)水中，濃度為(50±10)g/L。用PH試紙?jiān)?5℃時(shí)測(cè)定試驗(yàn)溶液的PH值為6.5~7.5。超出范圍時(shí)可加入分析純鹽酸或氫氧化鈉溶液進(jìn)行調(diào)整，配制好的溶液需經(jīng)過濾后方可使用。

B.醋酸—鹽霧溶液的配制

先將符合GBl266化學(xué)純的氯化鈉溶解于符合GB6682三級(jí)水中，濃度為(50±10)g／L然后用醋酸調(diào)節(jié)溶液的PH值，使其在3.1～3.3范圍內(nèi)，該P(yáng)H值用所收集的鹽霧樣品測(cè)得。應(yīng)在25℃時(shí)進(jìn)行PH值測(cè)量，配制好的溶液需經(jīng)過濾后方可使用。

C.銅加速的醋酸/鹽霧溶液的配制

第一步將符合GBl266化學(xué)純的氯化鈉溶液于符合GB6682三級(jí)水中，濃度為(50±10)g/L。第二步在3.8升的鹽水中加入試劑級(jí)的二氯化銅(CuCl221120)進(jìn)行溶解充分混合。第三步用醋酸調(diào)節(jié)溶液的PH值，使其在3.1~3.3范圍內(nèi)，該P(yáng)H值用所收集的鹽霧樣品測(cè)得。應(yīng)在25℃時(shí)進(jìn)行PH值測(cè)量，配制好的溶液需經(jīng)過濾后方可使用。

試驗(yàn)樣板的制備、養(yǎng)護(hù)及預(yù)處理

除另有規(guī)定外，可按GB/T1765－79(89)《測(cè)定耐濕熱、耐鹽霧、耐候性(人工加速)的漆膜制備法》的規(guī)定制備和養(yǎng)護(hù)樣板，被測(cè)樣板的背面及周邊可用被測(cè)產(chǎn)品或比被測(cè)產(chǎn)品更耐腐蝕的涂層體系涂覆。如做劃線試驗(yàn)時(shí)，可用一種具有碳化鎢刀尖的劃線工具與樣板表面接觸，劃出一條均勻的、劃穿底材上所有有機(jī)涂層的不帶毛刺的V字型切口的亮線。如需做劃穿金屬鍍層的試驗(yàn)，其劃穿程度應(yīng)由生產(chǎn)廠與用戶之間商定。如果用戶需要，經(jīng)商定也可劃出幾條線(交叉線、平行線)，劃線質(zhì)量可借助低倍放大鏡觀察。

樣板的投試、試驗(yàn)及檢查

養(yǎng)護(hù)期結(jié)束后的樣板留出一塊作標(biāo)準(zhǔn)板，其余3塊投入試驗(yàn)箱內(nèi)進(jìn)行曝露試驗(yàn)。樣板應(yīng)表面朝上放在樣板支架上，樣板之間及樣板與箱體之間均不允許接觸，且被測(cè)樣板不應(yīng)層疊放置，避免液滴從上層樣板濺落到下層樣板上影響試驗(yàn)結(jié)果。樣板在試板架上的排列應(yīng)以有規(guī)律的間隔時(shí)間改變，例如前排與中排及后排進(jìn)行交換。

鹽霧試驗(yàn)周期比較長(zhǎng)，一般是幾佰小時(shí)、1000h、2000h和4000h，甚至更長(zhǎng)時(shí)間也有采用。試驗(yàn)時(shí)間可參照相關(guān)產(chǎn)品標(biāo)準(zhǔn)的規(guī)定。因?yàn)闃?biāo)準(zhǔn)中規(guī)定每24h需檢查一次樣板，故試驗(yàn)時(shí)間一般為24h的倍數(shù)。但也可按美國(guó)ASTMD117-1997標(biāo)準(zhǔn)中推薦的曝露周期，即12，24，48，96，200，500，720h。

樣板的檢查及評(píng)定可按相關(guān)標(biāo)準(zhǔn)規(guī)定進(jìn)行，不劃線樣板的評(píng)定可參照GB/T1740－79《漆膜耐濕熱測(cè)定法》進(jìn)行，該標(biāo)準(zhǔn)中詳細(xì)規(guī)定了樣板的檢驗(yàn)項(xiàng)目如變色、起泡、生銹、脫落等及評(píng)級(jí)細(xì)則。檢查時(shí)一般采用目測(cè)法并借助透明材料制成的百分格進(jìn)行評(píng)判破壞程度及破壞面積，破壞程度分三個(gè)等級(jí)，其中1級(jí)最好．3級(jí)最差；

劃線樣板的評(píng)定可參照ASTMD1654－92《涂裝了色漆或涂料的試樣經(jīng)受腐蝕環(huán)境后的評(píng)定》進(jìn)行。標(biāo)準(zhǔn)中詳細(xì)規(guī)定了樣板的檢驗(yàn)項(xiàng)目，如：腐蝕斑點(diǎn)、起泡、自劃線漫延的腐蝕或涂層的損失(破壞程度)等。破壞程度分(0－10)個(gè)等級(jí)，其中10級(jí)最好，0級(jí)最差。

影響耐鹽霧試驗(yàn)結(jié)果的因素

1）鹽霧試驗(yàn)機(jī)及所有與鹽溶液或鹽霧接觸的部件都應(yīng)是惰性、不透氣的材料制成。否則部件的同步腐蝕將影響試板的檢驗(yàn)結(jié)果。

2）應(yīng)適當(dāng)調(diào)整噴霧塔的擋板角度，使噴嘴的噴射方向不會(huì)直接沖擊樣板。

3）鹽霧機(jī)的排空管應(yīng)有足夠的尺寸以降低箱內(nèi)回壓．排空管的末端也應(yīng)有遮擋，否則造成箱內(nèi)的壓力或真空的波動(dòng)。

4）為霧化鹽溶液而供給噴嘴的壓縮空氣應(yīng)作無(wú)油及無(wú)塵處理，否則容易將噴嘴堵塞并直接影響試驗(yàn)結(jié)果。

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